Abstract
Repeated wetting and drying is one of the most destructive actions that can induce continuous damage to in-situ rocks in many engineering applications. The situation is exacerbated if the action is coupled with flowing water conditions. In this work, the wet–dry (W–D) deterioration characteristics of gypsiferous rocks surrounding underground excavations were investigated. A series of tests at different W–D cycles with different flow rates (0, 10, and 20 l/h) were conducted on gypsiferous specimens to reveal the deterioration behaviors. The change in rock pore structure was characterized by nuclear magnetic resonance (NMR) method and the deterioration characteristics in its mechanical properties were investigated by the P-wave velocity test. Based on the disturbed state concept (DSC), a W–D deterioration model was established. The results showed that repeated W–D actions led to the formation of visible cracks which enhanced the dissolution of gypsiferous rocks, while the loose particles detached from the rock matrix were carried away by the flowing water, resulting in an uneven diameter reduction in the specimens. The damage of internal micro-porestructure and enlargement of internal pores were induced also by the combined action of the W–D processes and water flow. The feasibility of using the pore structure parameters to characterize the deterioration in the mechanical properties of gypsiferous rocks due to W–D actions at different water flow rates was demonstrated based on the proposed deterioration model. This study can provide a useful reference tool to help the engineering design of tunnels under similar geological conditions.
Highlights
-
A series of tests at different W-D cycles with different flow rates for the gypsiferous specimens were designed and conducted.
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The additional effect of groundwater flow on the cyclic W-D process and the W-D deterioration characteristics of gypsiferous rocks were revealed.
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A W-D deterioration model based on the disturbed state concept (DSC) was established to describe the damage of gypsiferous rocks caused by different W-D cycles.
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Abbreviations
- n :
-
Number of wet–dry cycles
- v :
-
Flow rates
- D F :
-
Average fractal dimension
- D Fi :
-
Fractal dimension of one of the surface contours of the specimen
- N a :
-
Number of counting boxes with the side length of a
- a :
-
Side length of the counting box
- k :
-
Photo number of the specimen
- S :
-
Pore surface area
- V :
-
Fluid volume
- T 2 :
-
Transverse relaxation time
- ρ 2 :
-
Surface relaxation strength of T2
- r :
-
Pore radius
- F S :
-
Pore-shape factor
- \(\phi^{0}\) :
-
Porosity at the initial stage
- \(\phi^{{\text{f}}}\) :
-
Porosity at the final stage
- \(\phi^{{\text{a}}}\) :
-
Apparent porosity
- D :
-
Disturbance factor (0 ≤ D ≤ 1)
- \(\phi^{{\text{a}}}(n,v)\) :
-
Growth function of apparent porosity
- \(\sigma\) :
-
Total stress (tangential stress or normal stress)
- \(\sigma_{{\text{i}}}\) :
-
Stress sustained by elements in RI state
- \(\sigma_{{\text{c}}}\) :
-
Stress by elements in FA state
- \(v_{{}}^{{\text{P}}}\) :
-
Apparent P-wave velocity
- \(v_{{\text{i}}}^{{\text{P}}}\) :
-
P-wave velocity of elements in RI state
- \(v_{{\text{c}}}^{{\text{P}}}\) :
-
P-wave velocity of elements in FA state
References
Dehestani A, Hosseini M, Beydokhti AT (2020) Effect of wetting-drying cycles on mode I and mode II fracture toughness of sandstone in natural (pH = 7) and acidic (pH = 3) environments. Theor Appl Fract Mech 107:102512. https://doi.org/10.1016/j.tafmec.2020.102512
Desai CS (2001) Mechanics of materials and interfaces: the disturbed state concept. CRC Press, Boca Raton
Dong ZC, Xia JW, Duan XM, Zhang ZX (2016) Pore structure of fine aggregate mortar based on the activity of calcined coal gangue from Xuzhou mining area. Rock Mech Rock Eng 35(4):819–825. https://doi.org/10.13722/j.cnki.jrme.2015.0620
Gutiérrez F, Calaforra JM, Cardona F, Ortí F, Durán JJ, Garay P (2008) Geological and environmental implications of evaporite karst in Spain. Environ Geol 53:951–965. https://doi.org/10.1007/s00254-007-0721-y
Hua W, Dong S, Peng F, Li K, Wang Q (2017) Experimental investigation on the effect of wetting-drying cycles on mixed mode fracture toughness of sandstone. Int J Rock Mech Min Sci 93:242–249. https://doi.org/10.1016/j.ijrmms.2017.01.017
James AN, Lupton ARR (1978) Gypsum and anhydrite in foundations of hydraulic structures. Géotechnique 28:249–272. https://doi.org/10.1680/geot.1978.28.3.249
Jamshidi A, Zamanian H, Zarei SR (2018) The effect of density and porosity on the correlation between uniaxial compressive strength and P-wave velocity. Rock Mech Rock Eng 51:1279–1286. https://doi.org/10.1007/s00603-017-1379-8
Jiang S, Huang M, Wu XZ, Chen ZF, Zhang KS (2021) Deterioration behavior of gypsum breccia in surrounding rock under the combined action of cyclic wetting-drying and flow rates. Bull Eng Geol Environ. https://doi.org/10.1007/s10064-021-02231-4
Kenyon WE, Takezaki H, Straley C, Sen PN, Herron M (1995) A laboratory study of nuclear magnetic resonance relaxation and its relation to depositional texture and petrophysical properties: carbonate Thamama group, mubarraz field, Abu Dhabi. Oil Field 2:477–502. https://doi.org/10.2118/29886-MS
Kim K, Franklin JA, Bowling AJ, Lecomte P, Palmer JHL (1999) International society for rock mechanics commission on testing methods. Int J Rock Mech Min Sci 24(1):53–73. https://doi.org/10.1016/0148-9062(87)91231-9
Klimchouk AB, Aksem SD (2005) Hydrochemistry and solution rates in gypsum karst: case study from the Western Ukraine. Environ Geol 48:307–319. https://doi.org/10.1007/s00254-005-1277-3
Li HB, Zhu JY, Guo HK (2008) Methods for calculating pore radius distribution in rock from NMR T2 spectra. Chin J Magn Reson 27:1512–1517
Li JL, Zhou KP, Ke B (2015) Association analysis of pore development characteristics and unconfined compressive strength property of granite under freezing thawing cycles. J Chin Coal Soc 40(8):1783–1789
Li BL, Lan JQ, Si GY, Lin GP, Hu LQ (2020) NMR-based damage characterisation of backfill material in host rock under dynamic loading. Int J Min Sci Technol 30(3):329–335. https://doi.org/10.1016/j.ijmst.2020.03.015
Lin B, Cerato AB (2014) Applications of SEM and ESEM in microstructural investigation of shale-weathered expansive soils along swelling-shrinkage cycles. Eng Geol 177:66–74. https://doi.org/10.1016/j.enggeo.2014.05.006
Liu L, Fang Z, Qi C, Zhang B, Guo L, Song KI (2018) Experimental investigation on the relationship between pore characteristics and unconfined compressive strength of cemented paste backfill. Constr Build Mater 179:254–264. https://doi.org/10.1016/j.conbuildmat.2018.05.224
Lu ZY, Sun YY (2010) Research on dimension algorithms about fractal of micro-structure curve of rock by using box-counting dimension method. In: 2010 International conference on intelligent system design and engineering application (ISDEA 2010), pp 189–192
Mahmut GD (2019) Identification of gypsum karstification using an electrical resistivity tomography technique: the case-study of the Sivas gypsum karst area (Turkey). Eng Geol 252:78–98. https://doi.org/10.1016/j.enggeo.2019.02.019
Mandelbrot BB (1967) How long is the coast of Britain? Statistical self-similarity and fractional dimension. Science 156(3775):636–638. https://doi.org/10.1126/science.156.3775.636
Qiang S, Zhang Y (2018) Combined effects of salt, cyclic wetting and drying cycles on the physical and mechanical properties of sandstone. Eng Geol 248:70–79. https://doi.org/10.1016/j.enggeo.2018.11.009
Sadeghiamirshahidi M, Vitton SJ (2019) Laboratory study of gypsum dissolution rates for an abandoned underground mine. Rock Mech Rock Eng 52:2053–2066. https://doi.org/10.1007/s00603-018-1696-6
Sharma PK, Singh TN (2008) A correlation between p-wave velocity, impact strength index, slake durability index and uniaxial compressive strength. Bull Eng Geol Environ 67(1):17–22. https://doi.org/10.1007/s10064-007-0109-y
Standardization Administration of the People’s Republic of China (2009) GB/T23561 methods for determining the physical and mechanical properties of coal and rock. Standards Press of China, Beijing
Sun W, Hou KP, Yang ZQ, Wen YY (2017) X-ray CT three-dimensional reconstruction and discrete element analysis of the cement paste backfill pore structure under uniaxial compression. Constr Build Mater 138:69–78. https://doi.org/10.1016/j.conbuildmat.2017.01.088
Taylor RK, Spears DA (1970) The breakdown of British coal measure rock. Int J Rock Mech Min Sci Geomech Abstr 7(5):481–501. https://doi.org/10.1016/0148-9062(70)90002-1
Torres-Suarez MC, Alarcon-Guzman A, Berdugo-De MR (2014) Effects of loading–unloading and wetting-drying cycles on geomechanical behaviors of mudrocks in the Colombian Andes. J Rock Mech Geotech Eng 6(3):257–268. https://doi.org/10.1016/j.jrmge.2014.04.004
Véhel JL, Legrand P (2004) Signal and image processing with FracLab. In: FRACTAL04, complexity and fractals in nature, 8th international multidisciplinary conference, pp 321–322
Vergara MR, Triantafyllidis T (2015) Swelling behavior of volcanic rocks under cyclic wetting and drying. Int J Rock Mech Min Sci 80:231–240. https://doi.org/10.1016/j.ijrmms.2015.08.021
Wang ZJ (2016) Damage evolution characteristics and the accumulation damage model of sandstone under dry–wet cycle. Dissertation, Chongqing University
Wang MF (2018) Analysis the deterioration mechanism and characteristics of drying-wetting cycles on gypsum rock. Dissertation, China University of Geosciences
Wang LL, Bornert M, Heripre E, Yang DS, Chanchole S (2014) Irreversible deformation and damage in argillaceous rocks induced by wetting/drying. J Appl Geophys 107(8):108–118. https://doi.org/10.1016/j.jappgeo.2014.05.015
Weng L, Wu ZJ, Li XB (2018) Mesodamage characteristics of rock with a pre-cut opening under combined static-dynamic loads: a nuclear magnetic resonance (NMR) investigation. Rock Mech Rock Eng 51:2339–2354. https://doi.org/10.1007/s00603-018-1483-4
Wu F, Qi S, Lan H (2005) Mechanism of uplift deformation of the dam foundation of Jiangya Water Power Station, Hunan Province, P. R. China. Hydrogeol J 13(3):451–466. https://doi.org/10.1007/s10040-004-0374-9
Xie KN, Jiang DY, Sun ZG, Chen J, Zhang WG, Jiang X (2018) NMR, MRI and AE statistical study of damage due to a low number of wetting-drying cycles in sandstone from the three gorges reservoir area. Rock Mech Rock Eng 51:3625–3634. https://doi.org/10.1007/s00603-018-1562-6
Zeng ZX, Kong LW, Wang M, Wang JT (2020) Effects of remoulding and wetting-drying-freezing-thawing cycles on the pore structures of Yanji mudstones. Cold Reg Sci Technol 174:103037. https://doi.org/10.1016/j.coldregions.2020.103037
Zhang Z, Jiang Q, Zhou C, Liu X (2014) Strength and failure characteristics of Jurassic Red-Bed sandstone under wetting–drying cycles conditions. Geophys J Int 198(2):1034–1044. https://doi.org/10.1093/gji/ggu181
Zhou KP, Li JL, Xu YJ, Zhang YM, Yang PQ, Chen LP (2012) Experimental study of NMR characteristics in rock under freezing and thawing cycles. Chin J Rock Mech Eng 43(12):4796–4800
Zhou K, Hu Z, Li J, Gao F, Wang M (2014) Study of marble damage evolution laws under unloading conditions based on nuclear magnetic resonance technique. Chin J Rock Mech Eng 33(S2):3523–3530. https://doi.org/10.13722/j.cnki.jrme.2014.s2.016
Zhou Z, Cai X, Chen L, Cao W, Zhao Y, Xiong C (2017) Influence of cyclic wetting and drying on physical and dynamic compressive properties of sandstone. Eng Geol 220:1–12. https://doi.org/10.1016/j.enggeo.2017.01.017
Acknowledgements
This work was supported by the National Natural Science Foundation of China (Grant No. 41972276), the Natural Science Foundation of Fujian Province (Grant No. 2020J06013) and the “Foal Eagle Program” Youth Top-notch Talent Project of Fujian Province (Grant No. 00387088). Their financial support is gratefully acknowledged.
Funding
Ming Huang (the second author) is grateful for the financial support of the National Natural Science Foundation of China (Grant No. 41972276), the Natural Science Foundation of Fujian Province (Grant No. 2020J06013) and the “Foal Eagle Program” Youth Top-notch Talent Project of Fujian Province (Grant No. 00387088).
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All authors participated in the design and conceptual study of this work. The experiment was mainly conducted by SJ and BL. The analysis of test results was performed by SJ and MH. The first draft of the manuscript was completed by SJ and MH. The manuscript was reviewed and revised by MH, YJ and CX. All authors read and approved the final manuscript.
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Jiang, S., Huang, M., Jiang, Y. et al. NMR-Based Investigation on the Wet–Dry Deterioration Characteristics of Gypsiferous Rocks Surrounding Underground Excavations. Rock Mech Rock Eng 55, 2323–2339 (2022). https://doi.org/10.1007/s00603-022-02780-4
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DOI: https://doi.org/10.1007/s00603-022-02780-4