CN103130570A - Method for preparing composite nitrogen fertilizer synergistic agent PBP by using banana pseudo-stem, and PBP application method - Google Patents
Method for preparing composite nitrogen fertilizer synergistic agent PBP by using banana pseudo-stem, and PBP application method Download PDFInfo
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- CN103130570A CN103130570A CN2013100600326A CN201310060032A CN103130570A CN 103130570 A CN103130570 A CN 103130570A CN 2013100600326 A CN2013100600326 A CN 2013100600326A CN 201310060032 A CN201310060032 A CN 201310060032A CN 103130570 A CN103130570 A CN 103130570A
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Abstract
The invention relates to a method for preparing a g composite nitrogen fertilizer synergistic agent PBP by using banana pseudo-stem. According to the invention, residual pseudo-stems and leaves after banana harvesting are chopped and instantly processed; the pseudo-stems and leaves are squeezed by using a squeezer, such that juice is obtained; residual slag in the juice is removed by filtering; an extracting agent is added into the rest juice, and the mixture is sufficiently mixed; precipitation is carried out; the clear solution is removed, and precipitate is collected; a stabilizing agent is added into the precipitate, the mixture is uniformly mixed, and centrifugal concentration is carried out; bake-drying is carried out, such that powdery PBP is obtained. The method for applying PBP as nitrogen fertilizer synergistic agent comprises the steps that: 5-20wt% of the composite nitrogen fertilizer synergistic agent PBP and 0.4-1wt% of dicyandiamide are added into a nitrogen fertilizer; the mixture is mixed, and can be applied. With the composite nitrogen fertilizer synergistic agent provided by the invention, nutrients such as zinc, iron, magnesium, and copper can be provided; soil and plant nutrition can be balanced; plant absorption of nitrogen nutrient can be promoted; and dual effects of urease inhibitor and nitrification inhibitor are provided.
Description
Technical field
The present invention relates to ornamental plant cultivation technique field, especially relate to a kind of method that banana caulo makes compound nitrogen fertilizer synergist PBP and using method of PBP utilized.
Background technology
Banana is Chinese the fifth-largest fruit, and banana area in 2009 and output are respectively 33.9 ten thousand hectares, 883.4 ten thousand tons of (China's Agricultural commodity yearbooks, 2011), simultaneously, the plantation banana also produces the approximately banana stem leaves of 3,051 ten thousand t, is a kind of very important Biological resources.But for a long time, banana stem leaves fails to obtain reasonable development, but abandon in the field, not only wasted resource but also contaminate environment.In fact, the tannin and the polyphenols that enrich in banana stem leaves juice are good nitrogen fertilizer potentiating agent work materials.
Nitrogenous fertilizer is the indispensable element of agriculture production, China has become world's nitrogenous fertilizer and has consumed the first big country at present, Chinese nitrogenous fertilizer consumption in 2010 be about 4,151 ten thousand tons (pure, lower same), under the at present popular fertilizing method of China, the utilization rate of nitrogen fertilizer of China only has 30%～35% (Geng Zhenguo, 2012), therefore, Chinese loss of nitrogen fertilizer amount was about 2,900 ten thousand tons in 2010, and this has not only greatly wasted resource, simultaneously, also accelerate the acidifying of soil, caused underground water, surface water pollution (Wang Zenong, 2010).
As a rule, denitrification and ammonia volatilization are main loss access, therefore, can control the conversion process of different nitrogenous fertilizer in soil by adding the nitrogen fertilizer potentiating agents such as nitrification inhibitor and urease inhibitor, thereby improve fertilizer utilization efficiency.
Nitrogen fertilizer potentiating agent substantially can be divided into chemosynthesis class and vegetable material and extract class.The chemosynthesis class has hydroquinone (HQ), two hydrogen by polymer substances such as (DCD), 2-amino-4-chloro-6-picoline (AM), N-serve (CP), 0-phenyl phosphoryl diamine (PPD), the cruel triamines of N-butyl sulfo-(BTPT), it is difficult to decomposition and produces residual and accumulation in soil, and contaminate environment is very careful in actual applications.And natural material class nitrogen fertilizer potentiating agent has " green " property, can overcome the negative impact of chemosynthesis class synergistic agent, the patent that present domestic existing publication No. is CNIO1844948A, be that a kind of natural plant material prints the application of element as nitrogen fertilizer potentiating agent of remonstrating with, it remonstrates with element as nitrogen fertilizer potentiating agent with the natural plant material seal, the seal that adds 1～10wt% in the nitrogenous fertilizer element of remonstrating with makes stable nitrogenous fertilizer.In addition, also having publication number is patent-natural plant-carrying compound nitrogen fertilizer synergistic of CN1454880A, its with Leaf of Lemon Eucalyptus, eucalyptus leaves or leaf of tea tree dry powder as plant urease inhibitor, and with the seeds of a tung oil tree dregs of rice, Leaf of Camphortree or Sweetscented Oleander Leaf powder mixture as plant-nitration inhibitor.
Summary of the invention
The object of the invention is to design a kind of method of utilizing banana caulo to make compound nitrogen fertilizer synergist PBP and this compound nitrogen fertilizer synergist of use PBP, address the above problem.
To achieve these goals, the technical solution used in the present invention is as follows:
A kind of method of utilizing banana caulo to make compound nitrogen fertilizer synergist PBP comprises that step is as follows:
The first step, processing immediately after the false stem under residual after banana results and leaf are cut down;
Second step, described false stem and leaf with after squeezing machine squeezing processing roll taking juice;
In the 3rd step, the residue in the described juice of elimination, remaining described juice add extraction agent and fully stir evenly, and precipitate parsing, discard clear liquid, stay the precipitation part;
The 4th step added the stablizer mixing in described precipitation, and then centrifugal concentrating, dry, and can obtain the banana caulo sap extraction material of powdery, i.e. compound nitrogen fertilizer synergist PBP.
In the described the first step, comprise the withered and rotten part of removing in described false stem and leaf, also comprise described false stem and leaf are carried out the stripping and slicing processing.
In the described the first step, also comprise and described false stem and leaf are cut into the wide * of about long * is high is the bulk of 2cm*5cm*30cm.
In described the 3rd step, precipitate and resolved about 10 hours;
Described the 4th step adds the stablizer mixing in described precipitation, and then centrifugal concentrating, dry under 50 ℃.
In described the 3rd step, described extraction agent comprises ferric sulfate, sal epsom, Tai-Ace S 150, copper sulfate, zinc sulfate, copper sulfate, iron(ic) chloride and calcium chloride; The concentration of wherein said ferric sulfate, described zinc sulfate and described copper sulfate is respectively 2.5%～5%, and the concentration of described iron(ic) chloride is 4%～6%.
The extraction yield of described extraction agent changes with extraction agent kind and leaching process pH condition:
| Extraction agent | Al 3+ | Zn 2+ | Fe 3+ | Mg + | Ba + | Ca + | Al 3+Zn 2+ |
| Minimum pH | 5.1 | 5.6 | 6.6 | 7.1 | 7.6 | 8.5 | 5.5 |
| Extraction yield | 10.5 | 10.4 | 8.8 | 8.1 | 7.4 | 7.0 | 87. |
The pH of described extraction agent is 5.5～6.0.
In described the 3rd step, add described extraction agent in remaining described juice after, improve preferably weak base of juice pH value basic cpd used;
In described the 3rd step, add described extraction agent in remaining described juice after, if can not in time carry out follow-up extraction procedure, need add the mountain sour potassium of plough fresh-keeping, add-on is 8g/25L juice.
The described compound nitrogen fertilizer synergist PBP that a kind of utilization makes is as the using method of nitrogen fertilizer potentiating agent: calculate with pure N mass content in nitrogenous fertilizer, add the described compound nitrogen fertilizer synergist PBP of 5～20wt% in nitrogenous fertilizer, 0.4 the Dyhard RU 100 of～1wt% is used after mixing.
Described using comprises that making base manure uses and/or do to topdress and use; Described nitrogenous fertilizer is urea, ammonium sulfate, ammonium chloride and/or bicarbonate of ammonia.
The so-called PBP of the present invention is the abbreviation of polyphenols of bananapseudostem.
The so-called Dyhard RU 100 of the present invention, English dicyandiamide is referred to as DCD.
The object of the present invention is to provide a kind of method of utilizing banana caulo to make compound nitrogen fertilizer synergist PBP and this compound nitrogen fertilizer synergist of use PBP, this natural plant material is nontoxic, cost is low, can obviously improve the chemical nitrogen fertilizer utilization ratio.
Beneficial effect of the present invention can be summarized as follows:
1, the present invention is along with the difference of extraction agent, and this compound nitrogen fertilizer synergist can provide the nutritive substances such as zinc, iron, magnesium, copper, thereby the nutrition of balance soil and plant is conducive to plant to the absorption of nitrogen nutrition.
2, the present invention studies and finds that compound nitrogen fertilizer synergist PBP has the double effects of urease inhibitor and nitrification inhibitor, can effectively delay acyl ammonium fertilizer and the conversion of ammonium fertilizer in soil, thus the losses such as the volatilization after minimizing nitrogenous fertilizer transforms and leaching.
3, the present invention's vegetable material used is from natural, aboundresources, and reproducibility is strong; Products production is with low cost, nontoxic, use safety, and is easy and simple to handle, can directly execute with multiple nitrogenous fertilizer is mixed.
Embodiment
In order to make technical problem solved by the invention, technical scheme and beneficial effect clearer, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, is not intended to limit the present invention.
A kind ofly utilize banana caulo to make compound nitrogen fertilizer synergist PBP and use the method for this compound nitrogen fertilizer synergist PBP, comprising that step is as follows: the first step, processing immediately after the false stem under residual after the banana results and leaf are cut down; Second step, described false stem and leaf with after squeezing machine squeezing processing roll taking juice; In the 3rd step, the residue in the described juice of elimination, remaining described juice add extraction agent and fully stir evenly, and precipitate parsing, discard clear liquid, stay the precipitation part; The 4th step added the stablizer mixing in described precipitation, and then centrifugal concentrating, dry, and can obtain the banana caulo sap extraction material of powdery, i.e. compound nitrogen fertilizer synergist PBP.
In a preferred embodiment, in the described the first step, comprise the withered and rotten part of removing in described false stem and leaf, comprise that also described false stem and leaf are carried out stripping and slicing to be processed, described false stem and leaf are cut into the wide * of about long * is high is the bulk of 2cm*5cm*30cm.In described the 3rd step, precipitate and resolved about 10 hours; Described the 4th step adds the stablizer mixing in described precipitation, and then centrifugal concentrating, dry under 50 ℃.
In the embodiment that is more preferably, in described the 3rd step, described extraction agent comprises ferric sulfate, sal epsom, Tai-Ace S 150, copper sulfate, zinc sulfate, copper sulfate, iron(ic) chloride and calcium chloride; The concentration of wherein said ferric sulfate, described zinc sulfate and described copper sulfate is respectively 2.5%～5%, and the concentration of described iron(ic) chloride is 4%～6%.The pH of described extraction agent is 5.5～6.0.
The extraction yield of described extraction agent changes with extraction agent kind and leaching process pH condition:
| Extraction agent | Al 3+ | Zn 2+ | Fe 3+ | Mg + | Ba + | Ca + | Al 3+Zn 2+ |
| Minimum pH | 5.1 | 5.6 | 6.6 | 7.1 | 7.6 | 8.5 | 5.5 |
| Extraction yield | 10.5 | 10.4 | 8.8 | 8.1 | 7.4 | 7.0 | 87. |
In the embodiment that is more preferably, in described the 3rd step, add described extraction agent in remaining described juice after, improve preferably weak base of juice pH value basic cpd used; In described the 3rd step, add described extraction agent in remaining described juice after, if can not in time carry out follow-up extraction procedure, need add the mountain sour potassium of plough fresh-keeping, add-on is 8g/25L juice.
The described compound nitrogen fertilizer synergist PBP that a kind of utilization makes is as the using method of nitrogen fertilizer potentiating agent: calculate with pure N mass content in nitrogenous fertilizer, add the described compound nitrogen fertilizer synergist PBP of 5～20wt% in nitrogenous fertilizer, 0.4 the Dyhard RU 100 of～1wt% is used after mixing.Described using comprises that making base manure uses and/or do to topdress and use; Described nitrogenous fertilizer is urea, ammonium sulfate, ammonium chloride and/or bicarbonate of ammonia.
Embodiment 1: banana caulo extracting substance PBP is as the application of nitrogen fertilizer potentiating agent: add PBP73.6 part in 1000 parts of urea, DCD1.84 part, fully mixing is with the conversion of N element in soil in stable urea, and in product, PBP content is 16% of pure nitrogen level, and DCD content is 0.4% of pure nitrogen level.
Embodiment 2: banana caulo extracting substance PBP is as the application of nitrogen fertilizer potentiating agent: add PBP33.6 part in 1000 parts of ammonium sulfate, DCD0.84 part, fully mixing is with the conversion of N element in soil in stable urea, and in product, PBP content is 16% of pure nitrogen level, and DCD content is 0.4% of pure nitrogen level.
Embodiment 3: banana caulo extracting substance PBP is as the application of nitrogen fertilizer potentiating agent: banana caulo extracting substance PBP is as the application of nitrogen fertilizer potentiating agent: add PBP50 part in 1000 parts of urea, DCD5 part, fully mixing is with the conversion of N element in soil in stable urea, in product, PBP content is 10.87% of pure nitrogen level, and DCD content is 1.09% of pure nitrogen level.
Embodiment 4: banana caulo extracting substance PBP is as the application of nitrogen fertilizer potentiating agent: banana caulo extracting substance PBP is as the application of nitrogen fertilizer potentiating agent: add PBP22.83 part in 1000 parts of ammonium sulfate, DCD2.29 part, fully mixing is with the conversion of N element in soil in stable urea, in product, PBP content is 10.87% of pure nitrogen level, and DCD content is 1.09% of pure nitrogen level.
Test-results
Adopt the indoor cultivation method, take the Chemical Mixed Fertilizer that is added with PBP as nitrogenous source (embodiment 1-2), be treated to contrast with 2 times of amount urea/sulphur acid ammoniums processing not adding inhibitor and equivalent urea and the ammonium sulfate that adds DCD, the fertilizer amount (purity nitrogen) of processing is 0.125g/kg, between incubation period, soil moisture content remains on 60% of field capacity, cultivates at room temperature state, cultivates the rear period sampling measuring of beginning.
Subordinate list 2, subordinate list 3 results show, with urea, ammonium sulfate as nitrogenous source, soil ammonium-state concentration reduces gradually with the prolongation of incubation time, nitrate raises gradually with the prolongation of incubation time, but the time that adds the soil ammonium peak appearance of PBP processing obviously will be later than an applied nitrogen processing, this is to have suppressed the activity of soil urease due to the existence of inhibitor, has delayed the hydrolysis of urea.In addition, it is basic all lower than the only CK processing of applied nitrogen in each incubation time that PBP processes nitrified nitrogen in soil concentration, especially the most obvious in cultivation concluding time (the 49th day), this is to have suppressed the activity of nitrobacteria due to the existence of inhibitor, has delayed the conversion of ammonium nitrogen to nitric nitrogen.
Subordinate list 4 results show, PBP processes and obviously improved the fresh weight of Plantula Brassicae chinensis.
The extraction yield of subordinate list 1 different extraction agents and minimum pH value
| Extraction agent | Al 3+ | Zn 2+ | Fe 3+ | Mg + | Ba + | Ca + | Al 3+Zn 2+ |
| Minimum pH | 5.1 | 5.6 | 6.6 | 7.1 | 7.6 | 8.5 | 5.5 |
| Extraction yield | 10.5 | 10.4 | 8.8 | 8.1 | 7.4 | 7.0 | 87 |
The conversion of subordinate list 2 urea in soil
Annotate: also be provided with a processing of not using urea in test, it is as the deduction of background ammonium nitrogen and nitric nitrogen, and the data in above form are the result after the deduction background values.
The conversion of subordinate list 3 ammonium sulfate in soil
Annotate: also be provided with a processing of not using urea in test, it is as the deduction of background ammonium nitrogen and nitric nitrogen, and the data in above form are the result after the deduction background values.
Subordinate list 4PBP processes impact and the significance test of difference on the Plantula Brassicae chinensis fresh weight
| Process | Plant fresh weight/g. strain | 5% conspicuous level | 1% conspicuous level |
| CK | 13.0 | d | BC |
| PBP1 | 15.5 | c | B |
| PBP2 | 20.6 | b | A |
| PBP3 | 23.1 | a | A |
| PBP4 | 20.7 | b | A |
| DCD | 11.2 | d | C |
Annotate: testing fertilizer used is ammonium sulfate, and test period is 49 days.
More than by the detailed description of concrete and preferred embodiment the present invention; but those skilled in the art should be understood that; the present invention is not limited to the above embodiment; within the spirit and principles in the present invention all; any modification of doing, be equal to replacement etc., within protection scope of the present invention all should be included in.
Claims (10)
1. a method of utilizing banana caulo to make compound nitrogen fertilizer synergist PBP, is characterized in that, comprises that step is as follows:
The first step, processing immediately after the false stem under residual after banana results and leaf are cut down;
Second step, described false stem and leaf with after squeezing machine squeezing processing roll taking juice;
In the 3rd step, the residue in the described juice of elimination, remaining described juice add extraction agent and fully stir evenly, and precipitate parsing, discard clear liquid, stay the precipitation part;
The 4th step added the stablizer mixing in described precipitation, and then centrifugal concentrating, dry, and can obtain the banana caulo sap extraction material of powdery, i.e. compound nitrogen fertilizer synergist PBP.
2. the method for utilizing banana caulo to make compound nitrogen fertilizer synergist PBP according to claim 1, it is characterized in that: in the described the first step, comprise the withered and rotten part of removing in described false stem and leaf, also comprise described false stem and leaf are carried out the stripping and slicing processing.
3. the method for utilizing banana caulo to make compound nitrogen fertilizer synergist PBP according to claim 2 is characterized in that: in the described the first step, also comprise and described false stem and leaf are cut into the wide * of about long * is high is the bulk of 2cm*5cm*30cm.
4. the banana caulo that utilizes of stating is according to claim 1 made the method for compound nitrogen fertilizer synergist PBP, it is characterized in that: in described the 3rd step, precipitate and resolved about 10 hours;
Described the 4th step adds the stablizer mixing in described precipitation, and then centrifugal concentrating, dry under 50 ℃.
5. the banana caulo that utilizes of stating is according to claim 1 made the method for compound nitrogen fertilizer synergist PBP, it is characterized in that: in described the 3rd step, described extraction agent comprises ferric sulfate, sal epsom, Tai-Ace S 150, copper sulfate, zinc sulfate, copper sulfate, iron(ic) chloride and calcium chloride; The concentration of wherein said ferric sulfate, described zinc sulfate and described copper sulfate is respectively 2.5%～5%, and the concentration of described iron(ic) chloride is 4%～6%.
6. the banana caulo that utilizes of stating is according to claim 5 made the method for compound nitrogen fertilizer synergist PBP, and it is characterized in that: the extraction yield of described extraction agent changes with extraction agent kind and leaching process pH condition:
7. the banana caulo that utilizes of stating is according to claim 5 made the method for compound nitrogen fertilizer synergist PBP, and it is characterized in that: the pH of described extraction agent is 5.5～6.0.
8. the banana caulo that utilizes of stating is according to claim 1 made the method for compound nitrogen fertilizer synergist PBP, it is characterized in that: in described the 3rd step, add described extraction agent in remaining described juice after, improve preferably weak base of juice pH value basic cpd used;
In described the 3rd step, add described extraction agent in remaining described juice after, if can not in time carry out follow-up extraction procedure, need add the mountain sour potassium of plough fresh-keeping, add-on is 8g/25L juice.
9. one kind is utilized described compound nitrogen fertilizer synergist PBP that claim 1-8 makes as the using method of nitrogen fertilizer potentiating agent, it is characterized in that: calculate with pure N mass content in nitrogenous fertilizer, add the described compound nitrogen fertilizer synergist PBP of 5～20wt% in nitrogenous fertilizer, 0.4 the Dyhard RU 100 of～1wt% is used after mixing.
10. the method for utilizing banana caulo to make compound nitrogen fertilizer synergist PBP according to claim 1 is characterized in that: described using comprises that making base manure uses and/or do to topdress and use; Described nitrogenous fertilizer is urea, ammonium sulfate, ammonium chloride and/or bicarbonate of ammonia.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104326821A (en) * | 2014-10-31 | 2015-02-04 | 韦方华 | Banana stem and leaf organic fertilizer and production method thereof |
| CN104341199A (en) * | 2013-08-02 | 2015-02-11 | 佛山市舜天生物科技有限公司 | An organic-inorganic composite liquid fertilizer |
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2013
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| US6939829B1 (en) * | 1999-08-27 | 2005-09-06 | Robert John Watson | Plant and product treatment |
| CN1454880A (en) * | 2003-04-08 | 2003-11-12 | 西南农业大学 | Natural plant-carrying compound nitrogen fertilizer synergistic agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104341199A (en) * | 2013-08-02 | 2015-02-11 | 佛山市舜天生物科技有限公司 | An organic-inorganic composite liquid fertilizer |
| CN104326821A (en) * | 2014-10-31 | 2015-02-04 | 韦方华 | Banana stem and leaf organic fertilizer and production method thereof |
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Application publication date: 20130605 |